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【英文标准名称】:TestMethodforSulfurinGasolineandDieselFuelbyMonochromaticWavelengthDispersiveX-rayFluorescenceSpectrometry
【原文标准名称】:用单色波长色散X射线荧光光谱法测定汽油燃料和柴油燃料中硫的试验方法
【标准号】:ANSI/ASTMD7039-2007
【标准状态】:作废
【国别】:美国
【发布日期】:2007
【实施或试行日期】:2007-05-22
【发布单位】:美国国家标准学会(US-ANSI)
【起草单位】:ANSI
【标准类型】:()
【标准水平】:()
【中文主题词】:柴油;汽油;硫;测试;波长色散;X射线荧光;X射线荧光光谱法;X射线光度法
【英文主题词】:Dieselfuels;Gasoline;Sulphur;Testing;Wavelengthdispersive;X-rayfluorescence;X-rayfluorescencespectrometry;X-rayspectrometry
【摘要】:Thistestmethodcoversthedeterminationoftotalsulfurbymonochromatic,wavelength-dispersiveX-rayfluorescence(MWDXRF)spectrometryinsingle-phasegasolines,dieselfuels,andrefineryprocessstreamsusedtoblendgasolineanddiesel,atconcentrationsfrom2mg/kgto500mg/kg.TheprecisionofthistestmethodwasdeterminedbyaninterlaboratorystudyusingrepresentativesamplesoftheliquidsdescribedinandThepooledlimitofquantitation(PLOQ)wasestimatedtobe4mg/kg.Note1Volatilesamplessuchashigh-vapor-pressuregasolinesorlighthydrocarbonsmightnotmeetthestatedprecisionbecauseoftheevaporationoflightcomponentsduringtheanalysis.GasolinesamplescontainingoxygenatesmaybeanalyzedwiththistestmethodprovidedthematrixofthecalibrationstandardsiseithermatchedtothesamplematricesorthematrixcorrectiondescribedinAnnexA1isappliedtotheresults.TheconditionsformatrixmatchingandmatrixcorrectionareprovidedintheInterferencessection(Section5).Gasolinesanddieselswithsulfurcontentsabove500mg/kgcanbeanalyzedafterdilutionwithappropriatesolvent(see5.2).Theprecisionandbiasofsulfurdeterminationsondilutedsampleshasnotbeendeterminedandmaynotbethesameasshownforneatsamples(Section15).Whentheelementalcompositionofthesamplesdiffersignificantlyfromthecalibrationstandardsusedtopreparethecalibrationcurve,thecautionsandrecommendationinSection5shouldbecarefullyobserved.ThevaluesstatedinSIunitsaretoberegardedasthestandard.Thevaluesgiveninparenthesesareforinformationonly.Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.Forspecifichazardinformation,see3.1.
【中国标准分类号】:E31
【国际标准分类号】:75_160_20
【页数】:
【正文语种】:英语